Wang Zhao-yang
2012
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Journal
Chemical Research and Application
Abstract
The title compound 3-chloro-4-(dibenzylamino)-5-methoxy-2(5H)-furanone was synthesized in THF solution and characterized by FT-IR,UV-Vis,1H NMR,13C NMR,MS,elemental analysis and X-ray diffraction.The results showed that the title compound belonged to orthorhombic system with Pbca space group and cell parameter:a=15.891(16),b=11.126(11),c=19.778(19),α=β=γ=90°,V=3497(6) 3,Z=8,Dc=1.306 Mg/m3,μ=0.234 mm-1,F(000)=1440.In the molecular structure of the title compound,the two phenyl rings are nearly perpendicular to the planar furanone with dihedral angles of 89.38°and 88.19°.