Hu Miaolin
2009
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Journal
Journal of Wenzhou University
Abstract
A new 5-fluorouracil derivative,(5-fluoro-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl) methyl thiophene-2-carboxylate,has been synthesized.Its structure has been characterized by means of 1H NMR,13C NMR,IR.Single crystal was diffracted with X-ray to ascertain the crystal structure of the compound.And the thermal feature of the compound was analyzed.Crystal data are shown as following:monoclinic,space group P2/c,a=9.613 4(14),b=4.838 1(7),c=24.534(4),α=90°,β=97.289(3)°,γ=90°,Z=4,F(000)=552,R1= 0.061 6.