Christina M. J. Fox, S. Ley
Apr 28, 2003
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Journal
Organic Syntheses
Abstract
tert-Butyl acetothioacetate and its use in synthesis: 3-Acetyl-4-hydroxy-5,5-dimethylfuran-2(4H)-one intermediate: S-tert-butyl 3-oxobutanthioate intermediate: 1-Carbomethoxy-1-methylethyl 3-oxobutanoate. product: 3-Acetyl-4-hydroxy-5,5-dimethylfuran-2(5H)-one. Keywords: acylation; acylation; addition, to CO; annulation, heterocyclic-[5]; cyclization, condensation; ring opening reactions; transesterification; silver(I) trifluoroacetate; tetrahydrofuran; mercaptans, stench