A. Koskinen
Apr 22, 2013
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Abstract
[102308-32-7]; [95715-87-0]; [117833-92-8]; [133464-37-6] C11H19NO4 (MW 229.27) InChI = 1S/C11H19NO4/c1-10(2,3)16-9(14)12-8(6-13)7-15-11(12,4)5/h6,8H,7H2,1-5H3 InChIKey = PNJXYVJNOCLJLJ-UHFFFAOYSA-N (tert-butyl 4-formyl-2,2-dimethyloxazolidine-3-carboxylate) Physical Data: bp 83–88 °C/1 mmHg (S);1 67 °C/0.3 mmHg (R); d 1.06 g cm−3 at 25 °C; [α]D −90 (c 1, CHCl3) (S); [α]D +93.5 (c 1.00, CHCl3) (R). Form Supplied in: colorless liquid; widely available in both enantiomeric forms. Purification: vacuum distillation (1.0–1.4 mmHg) through a 10-cm Vigreux column. Handling, Storage, and Precautions: must be stored in a tightly closed container in a dry and well-ventilated cool place. Showed no signs of decomposition or racemization when stored at 5 °C for 9 months. May cause skin and eye irritation. No toxicity data available.