Juxian Wang, Mingliang Liu, Jue Cao
Nov 8, 2008
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Influential Citations
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Journal
Acta Crystallographica Section E: Structure Reports Online
Abstract
The title compound, C13H23N3O4, was prepared starting from ethyl N-benzyl-3-oxopiperidine-4-carboxylate through a nine-step reaction, including hydrogenation, Boc (tert-butoxycarbonyl) protection, methylation, oximation, hydrolysis, esterification and ammonolysis. In the crystal structure, molecules are linked by intermolecular N—H⋯O hydrogen bonds to form a porous three-dimensional network with solvent-free hydrophobic channels extending along the c axis.