Hong-Lin Zhu, Yueqing Zheng
Oct 12, 2011
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Journal
Journal of Chemical Crystallography
Abstract
AbstractThe title molecule crystallizes in the monoclinic space group P21/c, with a = 13.010(3), b = 5.562(1), c = 11.358(2) Å, β = 92.61(3)°. The 3-butene-1,2,3-tricarboxylic acid forms a hydrogen-bonded 2D (6,3) network that adopts a threefold 2D → 2D parallel interpenetrating sheets structure with a 63 topology, generated via the supramolecular assembly of the 3-butene-1,2,3-tricarboxylic acid nodes.Graphical AbstractThe 3-butene-1,2,3-tricarboxylic acid was synthesized and characterized by single-crystal X-ray diffraction, and the molecule forms a threefold interpenetration of hydrogen-bonded 2D supramolecular layers with (6,3) network.